Figure 2
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Structural and compositional characterization of MnFe_PBA synthesized under ambient and cryogenic conditions. (A–F) The XRD patterns and the Rietveld refinement of MnFe_PBA_RT w/o EG, MnFe_PBA_RT w EG and MnFe_PBA_Cryo_−10°C. The SEM images and the statistics of the particle size distribution of MnFe_PBA_RT w/o EG, MnFe_PBA_RT w EG and MnFe_PBA_Cryo_−10°C, respectively. (G) Transmission electron microscopy (TEM) image of MnFe_PBA_cryo_−10°C. The XPS fine scan of Mn 2p (H) and Fe 2p (I) spectra of MnFe_PBA_cryo_−10°C.
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